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A gas chromatographic method for the analysis of 2,2'-dichlorodiethyl sulfide (commonly known as Sulfur Mustard) that had been trapped in the solvent, diethyl phthalate is described. The method utilises the improved sensitivity and selectivity offered by the new Pulsed Flame Photometric Detector to detect routinely samples containing 0.25 µg/mL of su lfur mustard in diethyl phthalate. The method is capable of fast and reliable analysis of samples containing 0.25-5.0 µg/mL of sulfur mustard in diethyl phthalate. Quality con trol measures determined that the method calibration was still within 5% control limits after nearly 500 sample injections. G/mL samples of sulfur mustard in DEP (or 0.35 ng of sulfur mustard injected on column) was set as the final goal. Improved detection of sulfur mustard was achieved by utilising a new design of gas chromatography detector (Pulsed Flame Photometric Detector) which offers increased selectivity for sulfur (and phosphorous) detection and improvements in sensitivity of up to 2 orders of magnitude above that of a normal flame photometric detector.

The method developed was found to not only meet the stated sensitivity requirements, but also exhibit excellent repr oducibility. Quality control meas ures established that the method calibration stayed within the 5% deviation control limits after analysis of almost 500 samples. Mindmanager 9 0194 Core Keygen Mac.